Complete Assignment of H1 and C13 NMR Spectra of 1,2,4-Trisubstituted Pyrroles

Complete Assignment of H1 and C13 NMR Spectra of 1,2,4-Trisubstituted Pyrroles

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Baby Blankets 1,2,4-Trisubstituted pyrroles were synthesized with an original one-pot domino allylic amination/palladium-catalysed Sonogashira cross-coupling and heterocyclisation process.1H and 13C NMR spectra were assigned for twelve new compounds containing different substituents in positions 1 and 2, and a carboxylic Motorcycle acid or ester group in position 4.Each assignment was based on the combination of one, and two-dimensional experiments (APT, COSY, HMBC).